Persistence and pathway of glyphosate degradation in the coastal wetland soil of central Delaware

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Authors
Moller, Spencer R.
Campos, Marco A.
Rilling, Joaquin I.
Bakkour, Rani
Hollenback, Anthony J.
Jorquera, Milko A.
Jaisi, Deb P.
Profesor GuĆ­a
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Date
Datos de publicaciĆ³n:
10.1016/j.jhazmat.2024.135238
JOURNAL OF HAZARDOUS MATERIALS,Vol.477,2024
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Article
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Materia geogrƔfica
Abstract
Glyphosate is a globally dominant herbicide. Here, we studied the degradation and microbial response to glyphosate application in a wetland soil in central Delaware for controlling invasive species (Phragmites australis). We applied a two-step solid-phase extraction method using molecularly imprinted polymers designed for the separation and enrichment of glyphosate and aminomethylphosphonic acid (AMPA) from soils before their analysis by ultra-high-performance liquid chromatography (UHPLC) and Q Exactive Orbitrap mass spectrometry methods. Our results showed that approximately 90 % of glyphosate degraded over 100 d after application, with AMPA being a minor (<10 %) product. Analysis of glyphosate-specific microbial genes to identify microbial response and function revealed that the expression of the phnJ gene, which codes C-P lyase enzyme, was consistently dominant over the gox gene, which codes glyphosate oxidoreductase enzyme, after glyphosate application. Both gene and concentration data independently suggested that C-P bond cleavage-which forms sarcosine or glycine-was the dominant degradation pathway. This is significant because AMPA, a more toxic product, is reported to be the preferred pathway of glyphosate degradation in other soil and natural environments. The degradation through a safer pathway is encouraging for minimizing the detrimental impacts of glyphosate on the environment.
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